In several research fields, only a few milligrams of product are available at the end of the synthesis process. To verify the synthetized structures, heteronuclear multidimensional NMR experiments, like HSQCs or HMBCs, are required. Sensitivity is typically a limiting factor to run these methods in a reasonable measurement time. In this blog post, we investigate …
A chemist´s dream to have a fast and reliable analytical tool that does not require tedious sample preparation and is available within the lab for reaction analysis might have come true with the implementation of efficient solvent suppression methods on mobile benchtop NMR spectrometers. As these instruments use compact permanent magnets, they do not require …
In this blog post, we explore the performance of the Spinsolve Benchtop NMR spectrometers for the identification of phosphine ligands by 31P NMR. Moreover, we demonstrate that the sensitivity of the Spinsolve spectrometers is high enough to monitor the oxidation reaction of these ligands in real time. Phosphines and related phosphorus-containing compounds have been extensively …
Monitoring the oxidation of Phosphine ligands using 31P NMR Read More »
Come and visit our booth 1012Â at ACS Spring 2023 ! This must-attend conference provides a superior educational event for industrial, regulatory, government, and academic scientists seeking to learn about and discuss applications of NMR to pharmaceuticals, polymers, petroleum, food/agriculture, and plant production that are rarely discussed at other NMR meetings. This remarkable conference affords …
ACS Spring 2023 – March 26-30 – Indianapolis, IN & Hybrid Read More »
Magritek is participating at Pittcon 2023 in Philadelphia, Pennsylvania, USAÂ – March 18 – 22, 2023
What is PANIC? PANIC is truly a unique conference experience! This must-attend conference provides a superior educational event for industrial, regulatory, government, and academic scientists seeking to learn about and discuss applications of NMR to pharmaceuticals, polymers, petroleum, food/agriculture, and plant production that are rarely discussed at other NMR meetings.This remarkable conference affords its participants …
The 75th Anniversary Conference of the American Academy of Forensic Sciences The program committee is centered on the conference theme, “Science Works.” In the past few years, science and the scientific method have been under attack, denigrated, and dismissed. AAFS President Laura Fulginiti’s plan is to offer scientific content demonstrating that forensic science provides trustworthy, …
AAFS (American Academy of Forensic Science) Annual Scientific Meeting 2023 Read More »
Thanksgiving is just around the corner in the US, with the anticipated meal and the nap that follows. There have been several debates from where the sleepiness comes from after the Thanksgiving feast. Is it the copious amount of food, the warm-and-fuzzy feeling from being around families and friends, or the star-of-the-dinner-show turkey? There is …
The quantification of the ingredients of a complex formulation by NMR spectroscopy is sometimes limited by the overlapping of the signals of the multiple compounds present in the product. The situation is particularly complicated when the sample contains molecules with high molecular weight. Macromolecules have broad resonances that cover large fractions of the spectrum and …
Unmask the NMR spectra of small molecules in complex formulations Read More »
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