Blog posts by mauricio

Small Molecule NMR Conference – September 22nd-25th, 2019 – Porto Portugal.

August 8th, 2019, by

SMASH is Celebrating its 20th Anniversary in 2019!

Magritek is participating in the SMASH 2019 on 22-25 September 2019 in Porto-Portugal. You’ll get a chance to meet us, learn about our company and we’ll get you acquainted with Spinsolve – high-performance benchtop NMR spectrometer that offers impressive sensitivity and resolution, it is robust and easy to use. We are looking forward to seeing you at this conference !!!

The Venue :

This year’s conference will be held at the Sheraton Porto Hotel & Spa from Sunday 22nd through Wednesday 25th, September 2019.

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POPs 2019 – International Symposium on Porous Organic Polymer – 9th-12th September – Heidelberg, Germany.

August 8th, 2019, by

Magritek is delighted to announce its participation in the POPs 2019 – International Symposium on Porous Organic Polymer – 9-12 September – Heidelberg, Germany in Heidelberg, Germany. You will have the chance to talk to our scientists about the capabilities and applications of the Spinsolve Benchtop NMR system. We are looking forward to seeing you at this event!

The venue:

 

 

SCS Fall Meeting 2019 – University of Zurich, Irchel Campus – 6th September 2019

August 8th, 2019, by

Magritek is excited to announce that we will be participating at the SCS Fall Meeting 2019 – which is being held at University of Zurich, Irchel Campus – 6th September 2019.

Magritek will have a live Spinsolve system running experiments, we would love for you to visit us and talk to our team about the capabilities and applications of our latest Spinsolve Benchtop NMR Systems.

We look forward to seeing you at this event!

 

 

20TH Annual Raps Meeting (RAPS 2019) will be held at the University of Leeds from 4-6th September 2019

August 8th, 2019, by

Magritek is delighted to announce its participation in the 20th Annual RAPS Meeting (RAPS 2019) will be held at the University of Leeds from 4-6th September 2019 and organized by Dr Nicholas Warren.. Please stop at our booth and talk to our scientists about the capabilities and applications of the  Spinsolve Benchtop NMR system. Our applications and support team will have a live, working Spinsolve Benchtop NMR.

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Mechanistic processes in organometallic chemistry Faraday Discussion – 2 – 4 September 2019, York, United Kingdom.

August 8th, 2019, by

Magritek is delighted to announce its participation in the Mechanistic processes in organometallic chemistry Faraday Discussion on  2 – 4 September 2019, York, United Kingdom. Please stop at our booth and talk to our scientists about the capabilities and applications of the  Spinsolve Benchtop NMR system. Our applications and support team will have a live, working Spinsolve Benchtop NMR.

Venue :

National STEM Learning Centre – National STEM Learning Centre, University of York, Heslington, York, YO190 5DD, United Kingdom

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SuniChem 2019 – AMU Saint Charles Amphitheater – 26th September Marseille-France

August 8th, 2019, by

Interfacing organic chemistry and flow chemistry

Magritek is delighted to announce its participation in the SuniChem 2019 in Marseille, France. Te SunniChem 2019 it’s organized by Aix Marseille Université and Sanofi and Magritek will participate as a partner.

Why SuniChem ?

  • Interfaces are sources of innovation
  • Technical experts benefit from networks
  • Magritek fosters tight links with Universities

ISMAR EUROMAR – Berlin, Germany, 25 to 30 August 2019.

June 18th, 2019, by

Join Magritek at EUROMAR 2019 in Berlin, Germany from 25 to 30 August 2019. You’ll get a chance to meet us, learn about our company and we’ll get you acquainted with the  Spinsolve – high-performance benchtop NMR spectrometer that offers impressive sensitivity and resolution, it is robust and easy to use. We are looking forward to seeing you at this conference !!!

Magritek will be running a workshop on the Henry Ford Building, on Wednesday 28.08.2019 ( the Room number has to be confirmed ), for registration please contact Mauricio Ferreira – mauricio@magritek.com
Euroismar registration button

Venue:

The conference will be taking place on the Dahlem Campus of the Free University, in the southwest of Berlin. The address of the main conference venue is:

Henry Ford Building
Freie Universität Berlin
Garystraße 35
14195 Berlin-Dahlem

The address of the additional sites used during the conference is:

Harnack-Haus. The Conference Venue of the Max Planck Society
Ihnestraße 16-20
14195 Berlin

 

 

EuropaCat 2019 – Aachen, Germany,18 to 23 August 2019.

June 18th, 2019, by

Join Magritek at EuropaCat in Aachen, Germany from 18 to 23 August 2019. You’ll get a chance to meet us, learn about our company and we’ll get you acquainted with the  Spinsolve – high-performance benchtop NMR spectrometer that offers impressive sensitivity and resolution, it is robust and easy to use. We are looking forward to seeing you at this conference !!!

The conference will take place at Aachen, the “triple point of Europe”.

Eurogress Aachen
Monheimsallee 48
52062 Aachen

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Benchtop NMR characterisation of diethyl phthalate containing land leeches repellent

June 18th, 2019, by

In Vietnam, for the observation of animals in the jungle of the national park of Cat Tien (and in other parts of the country and in Asia), the rangers give the tourists leech socks and a repellent cream for land leeches to put on the socks. Land leeches are terrestrial blood-sucking worm-like parasites. Reading the cream container, I noticed that it contains diethyl phthalate (DEP). Out of curiosity, I dissolved some of the cream in CDCl3 and acquired a NMR spectrum with the Spinsolve 80 MHz benchtop NMR spectrometer.

The 1D 1H spectrum confirms that the cream is mainly composed of diethyl phthalate (Fig. 1, a). A zoom of the spectrum (Fig. 1, b) shows the presence of some additional compounds overlapping with the 13C satellite peaks of DEP (0.55% of the main peaks). To simplify the identification of the additional compounds present in the cream I acquired a 1D 1H spectrum using the carbon decoupling protocol available in the Spinsolve software (Fig. 1, c). This method removes the satellites from the spectra making it possible to detect compounds dissolved at concentration smaller than 1% with respect to DEP.

Typical excipients used in such creams are fatty acid mixtures from butter and/or oils, glycerol/glycine, alcohol (multiplet ~ 3.5 ppm, CH2-OH) and PEG based compounds (peak ~ 3.6 ppm) and even perfume(s).

In our case, the fatty acid peaks are easily recognized. The terminal methyl of fatty acids is observed in region F around 0.8 ppm, the aliphatic chain in region E and probably under the CH3 of DEP, and the olefinic protons of saturated fatty acids around 5.2 ppm in the region A. As no signal is observed around 2.8 ppm, the saturated fatty acids present in the cream are mono unsaturated. The singlet at 2.47 ppm (singlet C) could be a residual solvent like DMSO or 1,3-dioxan, common solvents contaminating cosmetic cream. To check this hypothesis, ~ 2 µL of solvent was added. If the cream contains the solvent, the integral of peak C would increase, but in our case new peaks were observed (data not show). Region B correspond to a CH3 group next to a (mono or di) substituted aliphatic. The area D could be a triplet with a J coupling of 7 Hz. These peaks probably belong to a perfume, where the additional peaks of the perfume molecule overlap with peaks of DEP.

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